January 25, 2021

Download Ebook Free A Practical Guide To Gas Analysis By Gas Chromatography

A Practical Guide to Gas Analysis by Gas Chromatography

A Practical Guide to Gas Analysis by Gas Chromatography
Author : John Swinley,Piet de Coning
Publisher : Elsevier
Release Date : 2019-06-28
Category : Science
Total pages :440
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A Practical Gas Analysis by Gas Chromatography provides a detailed overview of the most important aspects of gas analysis by gas chromatography (GC) for both the novice and expert. Authors John Swinley and Piet de Coning provide the necessary information on the selection of columns and components, thus allowing the reader to assemble custom gas analysis systems for specific needs. The book brings together a wide range of disparate literature on this technique that will fill a crucial gap for those who perform different types of research, including lab operators, separation scientists, graduate students and academic researchers. This highly practical, up-to-date reference can be consulted in the lab to guide key decisions about proper setup, hardware and software selection, calibration, analysis, and more, allowing researchers to avoid the common pitfalls caused by incorrect infrastructure. Shows, in detail, how valve configurations work, allowing readers to understand the building blocks of extremely complex systems Presents the complete infrastructure for setting up a gas analysis laboratory in a single source Includes a full chapter on practical analytical systems for analyzing various gas mixtures

Gas Chromatography and Mass Spectrometry: A Practical Guide

Gas Chromatography and Mass Spectrometry: A Practical Guide
Author : O. David Sparkman,Zelda Penton,Fulton G. Kitson
Publisher : Academic Press
Release Date : 2011-05-17
Category : Science
Total pages :632
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The second edition of Gas Chromatography and Mass Spectrometry: A Practical Guide follows the highly successful first edition by F.G. Kitson, B.S. Larsen, and C.N. McEwen (1996), which was designed as an indispensible resource for GC/MS practitioners regardless of whether they are a novice or well experienced. The Fundamentals section has been extensively reworked from the original edition to give more depth of an understanding of the techniques and science involved with GC/MS. Even with this expansion, the original brevity and simple didactic style has been retained. Information on chromatographic peak deconvolution has been added along with a more in-depth understanding of the use of mass spectral databases in the identification of unknowns. Since the last edition, a number of advances in GC inlet systems and sample introduction techniques have occurred, and they are included in the new edition. Other updates include a discussion on fast GC and options for combining GC detectors with mass spectrometry. The section regarding GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types has the same number of compound types as the original edition, but the information in each section has been expanded to not only explain some of the spectra but to also explain why certain fragmentations take place. The number of Appendices has been increased from 12 to 17. The Appendix on Atomic Masses and Isotope Abundances has been expanded to provide tools to aid in determination of elemental composition from isotope peak intensity ratios. An appendix with examples on "Steps to follow in the determination of elemental compositions based on isotope peak intensities" has been added. Appendices on whether to use GC/MS or LC/MS, third-party software for use in data analysis, list of information required in reporting GC/MS data, X+1 and X+2 peak relative intensities based on the number of atoms of carbon in an ion, and list of available EI mass spectral databases have been added. Others such as the ones on derivatization, isotope peak patterns for ions with Cl and/or Br, terms used in GC and in mass spectrometry, and tips on setting up, maintaining and troubleshooting a GC/MS system have all been expanded and updated. Covers the practical instruction necessary for successful operation of GC/MS equipment Reviews the latest advances in instrumentation, ionization methods, and quantitation Includes troubleshooting techniques and a variety of additional information useful for the GC/MS practitioner A true benchtop reference A guide to a basic understanding of the components of a Gas Chromatograph-Mass Spectrometer (GC-MS) Quick References to data interpretation Ready source for information on new analyses

Gas Chromatography and Mass Spectrometry

Gas Chromatography and Mass Spectrometry
Author : Fulton G. Kitson,Barbara S. Larsen,Charles N. McEwen
Publisher : Academic Press
Release Date : 1996-08-30
Category : Science
Total pages :381
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This guide provides, under one cover, a wealth of practical information designed to facilitate the effectiveness of the GC/MS user. Separation conditions for numerous compound types are provided along with derivatized and underivatized compounds. A section on how to interpret mass spectral data, an extensive correlation of ion masses and neutral losses with possible structures, and examples of mass spectra are provided to further aid structure determination. Also included are basic information on instrumentation, ionization methods, quantitation, tips on the operation of mass spectrometers, the best derivatization procedures for a variety of compound types, troubleshooting techniques, and a variety of other information found to be useful to the practicing user of GC/MS instrumentation. This guide would be immediately valuable to the novice as well as the experienced GC/MS user who may not have the breadth of experience covered in this book. Key Features * Condenses and organizes recent and essential information for new and experienced GC/MS users * Comprehensively indexed and referenced * Includes practical methods of analysis * Serves as a text reference for short practical courses on the subject

Gas Chromatography and Lipids

Gas Chromatography and Lipids
Author : William W. Christie
Publisher : Matreya
Release Date : 1989
Category : Gas chromatography
Total pages :307
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Basic Gas Chromatography

Basic Gas Chromatography
Author : Harold M. McNair,James M. Miller
Publisher : John Wiley & Sons
Release Date : 2011-09-20
Category : Science
Total pages :256
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The New Edition of the Well-Regarded Handbook on GasChromatography Since the publication of the highly successful first edition ofBasic Gas Chromatography, the practice of chromatography hasundergone several notable developments. Basic GasChromatography, Second Edition covers the latest in the field,giving readers the most up-to-date guide available, whilemaintaining the first edition's practical, applied approach to thesubject and its accessibility to a wide range of readers. The text provides comprehensive coverage of basic topics in thefield, such as stationary phases, packed columns and inlets,capillary columns and inlets, detectors, and qualitative andquantitative analysis. At the same time, the coverage also featureskey additions and updated topics including: Gas chromatography-mass spectrometry (GC-MS) Sampling methods Multidimensional gas chromatography Fast gas chromatography Gas chromatography analysis of nonvolatile compounds Inverse gas chromatography and pyrolysis gaschromatography Along with these new and updated topics, the references,resources, and Web sites in Basic Gas Chromatography have beenrevised to reflect the state of the field. Concise and fundamentalin its coverage, Basic Gas Chromatography, Second Editionremains the standard handbook for everyone from undergraduatesstudying analytical chemistry to working industrial chemists.

Practical Gas Chromatography

Practical Gas Chromatography
Author : Katja Dettmer-Wilde,Werner Engewald
Publisher : Springer
Release Date : 2014-11-05
Category : Science
Total pages :902
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Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.

Process Gas Chromatographs

Process Gas Chromatographs
Author : Tony Waters
Publisher : John Wiley & Sons
Release Date : 2020-04-28
Category : Technology & Engineering
Total pages :400
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A guide to the fundamentals of applied gas chromatography and the process gas chromatograph, with practical procedures for design and troubleshooting This comprehensive resource provides the theory that underpins a full understanding of the fundamental techniques of gas chromatography and the process analyzer. Without relying on complex mathematics, the book addresses hands-on applications of gas chromatographs within process industries. The author – a noted expert on the topic – details both the scientific information needed to grasp the material presented and the practical applications for professionals working in the field. Process Gas Chromatographs: Fundamentals, Design and Implementation comprises 15 chapters, a glossary of terms and a series of self-assessment questions and quizzes. This important resource: Describes practical procedures for design and troubleshooting Contains concise chapters that provide a structured course for advanced students in process engineering Reviews the fundamentals of applied gas chromatography Details the operation and maintenance of process gas chromatographs Offers a summary, and self-assessment questions, for every chapter Is written by an international expert in the field with extensive industry knowledge and teaching experience in courses on process sampling systems and gas chromatography Written for process analyzer engineers and technicians, application engineers, and industrial environmental engineers, Process Gas Chromatographs: Fundamentals, Design and Implementation offers an essential guide to the basics of gas chromatography and reviews the applications of process gas chromatographs in industry today.

Static Headspace-Gas Chromatography

Static Headspace-Gas Chromatography
Author : Bruno Kolb,Leslie S. Ettre
Publisher : John Wiley & Sons
Release Date : 2006-05-05
Category : Science
Total pages :384
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The only reference to provide both current and thorough coverage of this important analytical technique Static headspace-gas chromatography (HS-GC) is an indispensable technique for analyzing volatile organic compounds, enabling the analyst to assay a variety of sample matrices while avoiding the costly and time-consuming preparation involved with traditional GC. Static Headspace-Gas Chromatography: Theory and Practice has long been the only reference to provide in-depth coverage of this method of analysis. The Second Edition has been thoroughly updated to reflect the most recent developments and practices, and also includes coverage of solid-phase microextraction (SPME) and the purge-and-trap technique. Chapters cover: * Principles of static and dynamic headspace analysis, including the evolution of HS-GC methods and regulatory methods using static HS-GC * Basic theory of headspace analysis-physicochemical relationships, sensitivity, and the principles of multiple headspace extraction * HS-GC techniques-vials, cleaning, caps, sample volume, enrichment, and cryogenic techniques * Sample handling * Cryogenic HS-GC * Method development in HS-GC * Nonequilibrium static headspace analysis * Determination of physicochemical functions such as vapor pressures, activity coefficients, and more Comprehensive and focused, Static Headspace-Gas Chromatography, Second Edition provides an excellent resource to help the reader achieve optimal chromatographic results. Practical examples with original data help readers to master determinations in a wide variety of areas, such as forensic, environmental, pharmaceutical, and industrial applications.

The Troubleshooting and Maintenance Guide for Gas Chromatographers

The Troubleshooting and Maintenance Guide for Gas Chromatographers
Author : Dean Rood
Publisher : John Wiley & Sons
Release Date : 2007-09-24
Category : Science
Total pages :344
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This fourth edition of the classic guide for every user of gas chromatographic instrumentation is now updated to include such new topics as fast GC using narrow, short columns, electronic pressure control, and basic aspects of quantitative gas chromatography. The author shares his many years of experience in technical support for gas chromatography users, addressing the most common problems, questions and misconceptions in capillary gas chromatography. He structures and presents the material in a concise and practical manner, suitable even for the most inexperienced user without any detailed knowledge of chemistry or chromatography. For lab technicians in chemistry, analytical, food, medicinal and environmental chemists, pharmaceutists.

A Practical Guide to Compressor Technology

A Practical Guide to Compressor Technology
Author : Heinz P. Bloch
Publisher : John Wiley & Sons
Release Date : 2006-09-18
Category : Science
Total pages :590
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A Complete overview of theory, selection, design, operation, andmaintenance This text offers a thorough overview of the operatingcharacteristics, efficiencies, design features, troubleshooting,and maintenance of dynamic and positive displacement process gascompressors. The author examines a wide spectrum of compressorsused in heavy process industries, with an emphasis on improvingreliability and avoiding failure. Readers learn both the theoryunderlying compressors as well as the myriad day-to-day practicalissues and challenges that chemical engineers and plant operationpersonnel must address. The text features: Latest design and manufacturing details of dynamic and positivedisplacement process gas compressors Examination of the full range of machines available for theheavy process industries Thorough presentation of the arrangements, materialcomposition, and basic laws governing the design of all importantprocess gas compressors Guidance on selecting optimum compressor configurations,controls, components, and auxiliaries to maximize reliability Monitoring and performance analysis for optimal machinerycondition Systematic methods to avoid failure through the application offield-tested reliability enhancement concepts Fluid instability and externally pressurized bearings Reliability-driven asset management strategies forcompressors Upstream separator and filter issues The text's structure is carefully designed to build knowledgeand skills by starting with key principles and then moving to moreadvanced material. Hundreds of photos depicting various types ofcompressors, components, and processes are provided throughout. Compressors often represent a multi-million dollar investmentfor such applications as petrochemical processing and refining,refrigeration, pipeline transport, and turbochargers andsuperchargers for internal combustion engines. This text enablesthe broad range of engineers and plant managers who work with thesecompressors to make the most of the investment by leading them tothe best decisions for selecting, operating, upgrading,maintaining, and troubleshooting.

A Practical Guide to Geometric Regulation for Distributed Parameter Systems

A Practical Guide to Geometric Regulation for Distributed Parameter Systems
Author : Eugenio Aulisa,David Gilliam
Publisher : CRC Press
Release Date : 2015-06-18
Category : Mathematics
Total pages :294
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A Practical Guide to Geometric Regulation for Distributed Parameter Systems provides an introduction to geometric control design methodologies for asymptotic tracking and disturbance rejection of infinite-dimensional systems. The book also introduces several new control algorithms inspired by geometric invariance and asymptotic attraction for a wide range of dynamical control systems. The first part of the book is devoted to regulation of linear systems, beginning with the mathematical setup, general theory, and solution strategy for regulation problems with bounded input and output operators. The book then considers the more interesting case of unbounded control and sensing. Mathematically, this case is more complicated and general theorems in this area have become available only recently. The authors also provide a collection of interesting linear regulation examples from physics and engineering. The second part focuses on regulation for nonlinear systems. It begins with a discussion of theoretical results, characterizing solvability of nonlinear regulator problems with bounded input and output operators. The book progresses to problems for which the geometric theory based on center manifolds does not directly apply. The authors show how the idea of attractive invariance can be used to solve a series of increasingly complex regulation problems. The book concludes with the solutions of challenging nonlinear regulation examples from physics and engineering.

Mass Spectrometry-Based Metabolomics

Mass Spectrometry-Based Metabolomics
Author : Sastia Prama Putri,Eiichiro Fukusaki
Publisher : CRC Press
Release Date : 2016-04-21
Category : Science
Total pages :294
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Mass Spectrometry-Based Metabolomics: A Practical Guide is a simple, step-by-step reference for profiling metabolites in a target organism. It discusses optimization of sample preparation for urine, serum, blood, tissue, food, and plant and animal cell samples. Encompassing three different technical fields—biology, analytical chemistry, and informatics— mass spectrometry-based metabolomics can be challenging for biologists without special training in quantitative mass spectrometry. This book is designed to overcome this limitation by providing researchers with the knowledge they need to use metabolomics technology in their respective disciplines. The book summarizes all steps in metabolomics research, from experimental design to sample preparation, analytical procedures, and data analysis. Case studies are presented for easy understanding of the metabolomics workflow and its practical applications in different research fields. The book includes an in-house library and built-in software so that those new to the field can begin to analyze real data samples. In addition to being an excellent introductory text, the book also contains the latest advancements in this emerging field and can thus be a useful reference for metabolomics specialists.

Comprehensive Two Dimensional Gas Chromatography

Comprehensive Two Dimensional Gas Chromatography
Author : Lourdes Ramos
Publisher : Elsevier
Release Date : 2009-07-22
Category : Science
Total pages :328
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The book reviews the basic concepts and highlights the most relevant advances and developments that have taken place in the field of comprehensive two dimensional gas chromatography (GC x GC) since its introduction in 1991. The several instrumental and technical approaches assayed and developed during these seventeen years and that have contributed to the development of this powerful separation technique and to its increasing application in many areas is explained and comprehensively illustrated through a number of chapters devoted these specific topics. More specialized aspects of the technique, including theoretical aspects, modelization of the chromatographic process, software developments, and alternative couplings is also covered. Finally, special attention is paid to data treatment, for both qualitative and quantitative analysis. This book will be a practical resource that will explain from basic to specialized concepts of GC x GC and will show the current state-of-the-art and discuss future trends of this technique. Outlines basic concepts and principles of GCxGC technique for non-specialists to apply the technique to their research Provides detailed descriptions of recent technical advances and serves as an instructional guide in latest applications in GCxGC Sets the scene for possible future development and alternative new applications of technique

Flow Analysis

Flow Analysis
Author : Victor Cerda,Laura Ferrer,Jessica Avivar,Amalia Cerda
Publisher : Newnes
Release Date : 2014-01-13
Category : Science
Total pages :288
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Flow Analysis: A Practical Guide reviews flow techniques for automating chemical analysis with the goal of increasing efficiency and producing better analytical results. Various applications for flow techniques are reviewed including industrial process monitoring (for example, foods and beverages, drugs and pharmaceuticals); as well as agricultural, life science, radioactivity, and environmental analysis with an emphasis on the latter. This book is a valuable resource for young scientists or graduate-level students who want to learn how to introduce flow techniques into their experiments, and for experts who need specific and technical details to develop complete experimental systems. Includes descriptions of the theoretical and technical bases of the most important flow techniques Focuses on new trends in the field such as using flow techniques for radioactivity and environmental applications Features instructions for coupling different types of detectors online with flow systems

Gas Chromatography–Mass Spectrometry

Gas Chromatography–Mass Spectrometry
Author : Diane C Turner,Mathias Schäfer,Steven Lancaster,Imran Janmohamed,Anthony Gachanja,Jason Creasey
Publisher : Royal Society of Chemistry
Release Date : 2019-11-28
Category : Science
Total pages :319
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Gas chromatography–mass spectrometry (GC-MS) is a powerful way to analyse a range of substances. It is used in everything from food safety to medicine. It has even been used to protect endangered vultures through analysis of poisonous pesticide molecules in their environment! I want to apply this technique, where do I begin? Is GC-MS is the right technique to use? How do I prepare my samples and calibrate the instruments? This textbook has the answers to all these questions and more. Throughout the book, case studies illustrate the practical process, the techniques used and any common challenges. Newcomers can easily search for answers to their question and find clear advice with coloured images on how to get started and all subsequent steps involved in using GC-MS as part of a research process. Readers will find information on collecting and preparing samples, designing and validating methods, analysing results, and troubleshooting. Examples of pollutant, food, oil and fragrance analysis bring the theory to life. The authors use their extensive experience teaching GC-MS theory and practice and draw on their combined backgrounds applying the technique in academic and industry settings to bring this practical reference together. The authors also design and teach the Royal Society of Chemistry’s Pan Africa Chemistry Network GC-MS course, which is supported by GSK.